TA Instruments

AR1772-0001f

28/03/2013 12:00:40

Sample name	DI 40 mm AL blank plate 10 mm gap
Sample notes	 
Experiment notes	DI Deionised water, 40 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	mr1
Sample density	1.000 g/cm^3
Results file name	AR1772
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	28/03/2013 12:00:40

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	40 mm ETC AL plate with studs
Geometry notes	Standard ETC AL parallel plate with studs
Geometry material	Aluminum
Parallel plate diameter	40.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	2.056 micro N.m.s^2
Geometry compliance	3.130E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	2.000 
Shear stress factor	79580 1/m^3
Measurement system factor	39790 1/m^3
Fluid density factor	8.378E-10 m^5
Normal force factor	1592 1/m^2
Backoff distance	26500 micro m
Approximate sample volume	12.57 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	1
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.01 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0000	4.098	8.5681	10000	20.0	5.858	31.000	0.6818	8.196	0.08319	9324	1.6947	138.8	3.3894	338.94	3.411E-3	0.0	0.5
2.0000	9.983	11.721	10000	20.0	5.855	32.000	0.9327	19.97	0.04672	9319	13.4042	23.38	26.808	2680.8	3.411E-3	0.0	0.5
3.0000	15.54	22.248	10000	20.0	5.855	33.000	1.770	31.09	0.05695	9319	27.1283	9.643	54.257	5425.7	3.411E-3	0.1	0.6
4.0000	18.46	29.102	10000	20.0	5.857	34.000	2.316	36.93	0.06271	9321	40.9373	6.835	81.875	8187.5	3.411E-3	0.1	0.6
5.0120	24.70	44.924	10000	20.0	5.857	35.012	3.575	49.40	0.07237	9322	68.1845	3.820	136.37	13637	3.411E-3	0.1	0.6
6.0160	31.60	66.098	10000	20.0	5.855	36.016	5.260	63.20	0.08322	9319	106.8160	2.333	213.63	21363	3.411E-3	0.1	0.6
7.0200	34.04	74.599	10000	20.0	5.853	37.020	5.936	68.08	0.08719	9315	126.6360	2.010	253.27	25327	3.411E-3	0.1	0.6
8.0000	39.31	92.597	10000	20.0	5.850	38.000	7.369	78.63	0.09372	9310	165.3060	1.506	330.61	33061	3.411E-3	0.1	0.6
9.0160	46.04	116.77	10000	20.0	5.845	39.016	9.292	92.08	0.1009	9303	223.2540	1.097	446.51	44651	3.411E-3	0.2	0.7
10.016	50.96	137.60	10000	20.0	5.841	40.016	10.95	101.9	0.1074	9297	274.7960	0.8949	549.59	54959	3.411E-3	0.2	0.7
11.016	55.73	158.31	10000	20.0	5.836	41.016	12.60	111.5	0.1130	9288	326.0840	0.7477	652.17	65217	3.411E-3	0.2	0.7
12.016	60.10	178.26	10000	20.0	5.831	42.016	14.19	120.2	0.1180	9280	377.2770	0.6423	754.55	75455	3.411E-3	0.2	0.7
13.012	64.42	198.01	10000	20.0	5.829	43.012	15.76	128.8	0.1223	9277	434.8120	0.5589	869.62	86962	3.411E-3	0.2	0.7
14.012	69.15	223.59	10000	20.0	5.827	44.012	17.79	138.3	0.1286	9273	499.8130	0.4848	999.63	99963	3.411E-3	0.2	0.7
14.996	75.68	258.32	10000	20.0	5.821	44.996	20.56	151.4	0.1358	9264	594.2140	0.4043	1188.4	1.1884E5	3.411E-3	0.2	0.7
15.996	79.93	279.85	10000	20.0	5.814	45.996	22.27	159.9	0.1393	9254	664.2840	0.3621	1328.6	1.3286E5	3.411E-3	0.3	0.8
17.000	84.53	306.39	10000	20.0	5.812	47.000	24.38	169.1	0.1442	9249	740.6910	0.3236	1481.4	1.4814E5	3.411E-3	0.3	0.8
18.012	90.98	342.71	10000	20.0	5.802	48.012	27.27	182.0	0.1499	9234	855.0090	0.2789	1710.0	1.7100E5	3.411E-3	0.3	0.8
19.016	95.04	369.08	10000	20.0	5.799	49.016	29.37	190.1	0.1545	9229	931.2710	0.2555	1862.5	1.8625E5	3.411E-3	0.3	0.8
20.000	99.40	392.46	10000	20.0	5.796	50.000	31.23	198.8	0.1571	9225	1020.1900	0.2334	2040.4	2.0404E5	3.411E-3	0.3	0.8
21.016	105.8	436.36	10000	20.0	5.786	51.016	34.72	211.7	0.1641	9208	1153.6200	0.2056	2307.2	2.3072E5	3.411E-3	0.4	0.9
22.016	109.9	462.70	10000	20.0	5.781	52.016	36.82	219.8	0.1675	9201	1242.5400	0.1904	2485.1	2.4851E5	3.411E-3	0.4	0.9
23.012	114.2	488.64	10000	20.0	5.778	53.012	38.88	228.5	0.1702	9196	1343.6000	0.1762	2687.2	2.6872E5	3.411E-3	0.4	0.9
24.000	120.7	530.70	10000	20.0	5.766	54.000	42.23	241.3	0.1750	9177	1495.7200	0.1576	2991.4	2.9914E5	3.411E-3	0.4	0.9
25.024	124.7	567.20	10000	20.0	5.758	55.024	45.14	249.5	0.1809	9164	1597.0200	0.1472	3194.0	3.1940E5	3.411E-3	0.4	0.9
26.016	129.1	588.39	10000	20.0	5.754	56.016	46.82	258.1	0.1814	9157	1711.0900	0.1374	3422.2	3.4222E5	3.411E-3	0.4	0.9
27.016	135.5	640.73	10000	20.0	5.745	57.016	50.99	270.9	0.1882	9143	1882.7900	0.1246	3765.6	3.7656E5	3.412E-3	0.5	1.0
28.004	139.6	670.78	10000	20.0	5.741	58.004	53.38	279.1	0.1912	9138	1995.8300	0.1173	3991.7	3.9917E5	3.411E-3	0.5	1.0
29.016	143.6	695.49	10000	20.0	5.732	59.016	55.35	287.3	0.1926	9123	2116.1101	0.1105	4232.2	4.2322E5	3.411E-3	0.5	1.0
30.016	150.0	746.22	10000	20.0	5.721	60.016	59.38	300.1	0.1979	9104	2305.8799	0.1011	4611.8	4.6118E5	3.411E-3	0.5	1.0
30.996	154.2	780.53	10000	20.0	5.714	60.996	62.11	308.3	0.2015	9095	2432.4099	0.09568	4864.8	4.8648E5	3.411E-3	0.5	1.0
32.000	158.3	813.71	10000	20.0	5.711	62.000	64.75	316.5	0.2046	9090	2565.8301	0.09071	5131.7	5.1317E5	3.411E-3	0.5	1.0
33.016	164.7	863.91	10000	20.0	5.700	63.016	68.75	329.3	0.2088	9072	2773.7600	0.08365	5547.5	5.5475E5	3.411E-3	0.6	1.1
34.008	168.8	897.55	10000	20.0	5.688	64.008	71.42	337.6	0.2116	9053	2912.7200	0.07944	5825.4	5.8254E5	3.411E-3	0.6	1.1
34.996	174.9	950.47	10000	20.0	5.672	64.996	75.64	349.8	0.2162	9027	3130.0000	0.07379	6260.0	6.2600E5	3.411E-3	0.6	1.1
36.012	179.1	989.78	10000	20.0	5.671	66.012	78.76	358.2	0.2199	9025	3280.0300	0.07033	6560.1	6.5601E5	3.411E-3	0.6	1.1
37.012	183.3	1019.7	10000	20.0	5.659	67.012	81.15	366.5	0.2214	9007	3430.8101	0.06704	6861.6	6.8616E5	3.411E-3	0.6	1.1
38.000	189.4	1076.2	10000	20.0	5.643	68.000	85.64	378.8	0.2261	8981	3664.2900	0.06260	7328.6	7.3286E5	3.411E-3	0.6	1.1
39.012	193.6	1119.7	10000	20.0	5.639	69.012	89.10	387.3	0.2301	8975	3828.7100	0.05985	7657.4	7.6574E5	3.411E-3	0.7	1.2
40.016	199.8	1172.6	10000	20.0	5.626	70.016	93.31	399.6	0.2335	8955	4074.8799	0.05607	8149.8	8.1498E5	3.411E-3	0.7	1.2
41.000	203.8	1215.1	10000	20.0	5.619	71.000	96.69	407.7	0.2372	8943	4240.1699	0.05381	8480.3	8.4803E5	3.411E-3	0.7	1.2
41.996	208.0	1248.4	10000	20.0	5.610	71.996	99.34	416.0	0.2388	8928	4416.6802	0.05159	8833.4	8.8334E5	3.411E-3	0.7	1.2
43.000	214.2	1315.2	10000	20.0	5.593	73.000	104.7	428.5	0.2443	8902	4683.5601	0.04849	9367.1	9.3671E5	3.411E-3	0.7	1.2
44.008	218.3	1351.0	10000	20.0	5.591	74.008	107.5	436.5	0.2463	8898	4857.4702	0.04669	9715.0	9.7150E5	3.411E-3	0.7	1.2
44.996	224.4	1406.7	10000	20.0	5.572	74.996	111.9	448.8	0.2494	8868	5135.1899	0.04402	10270	1.0270E6	3.411E-3	0.7	1.2
45.996	228.5	1451.0	10000	20.0	5.571	75.996	115.5	457.1	0.2526	8867	5324.4302	0.04244	10649	1.0649E6	3.411E-3	0.8	1.3
47.016	234.6	1497.3	10000	20.0	5.551	77.016	119.1	469.3	0.2539	8835	5608.4702	0.04012	11217	1.1217E6	3.411E-3	0.8	1.3
47.996	238.8	1542.8	10000	20.0	5.554	77.996	122.8	477.5	0.2571	8840	5814.6699	0.03876	11629	1.1629E6	3.411E-3	0.8	1.3
48.996	242.9	1584.3	10000	20.0	5.540	78.996	126.1	485.9	0.2595	8817	6013.0698	0.03735	12026	1.2026E6	3.411E-3	0.8	1.3
49.996	249.0	1645.2	10000	20.0	5.527	79.996	130.9	498.0	0.2629	8797	6315.8701	0.03547	12632	1.2632E6	3.411E-3	0.8	1.3
51.012	253.1	1688.6	10000	20.0	5.513	81.012	134.4	506.1	0.2655	8774	6523.9399	0.03425	13048	1.3048E6	3.411E-3	0.9	1.4
52.016	259.3	1765.0	10000	20.0	5.486	82.016	140.5	518.5	0.2709	8731	6845.7998	0.03248	13692	1.3692E6	3.411E-3	0.9	1.4
53.008	263.3	1809.2	10000	20.0	5.479	83.008	144.0	526.6	0.2734	8720	7065.1602	0.03144	14130	1.4130E6	3.411E-3	0.9	1.4
54.012	267.3	1858.8	10000	20.0	5.468	84.012	147.9	534.6	0.2767	8703	7388.3301	0.03045	14777	1.4777E6	3.411E-3	0.9	1.4
55.016	273.5	1918.6	10000	20.0	5.459	85.016	152.7	547.0	0.2791	8688	7614.0898	0.02904	15228	1.5228E6	3.411E-3	0.9	1.4
55.996	277.6	1962.5	10000	20.0	5.432	85.996	156.2	555.1	0.2813	8645	7840.8101	0.02805	15682	1.5682E6	3.411E-3	0.9	1.4
56.996	283.6	2020.1	10000	20.0	5.427	86.996	160.8	567.1	0.2834	8637	8181.2500	0.02685	16363	1.6363E6	3.411E-3	0.9	1.4
57.996	287.7	2064.4	10000	20.0	5.428	87.996	164.3	575.3	0.2855	8639	8420.8604	0.02610	16842	1.6842E6	3.411E-3	1.0	1.5
59.000	293.8	2142.7	10000	20.0	5.406	89.000	170.5	587.6	0.2902	8604	8780.1504	0.02492	17560	1.7560E6	3.411E-3	1.0	1.5
60.012	297.8	2189.8	10000	20.0	5.400	90.012	174.3	595.6	0.2926	8594	9023.1699	0.02423	18046	1.8046E6	3.411E-3	1.0	1.5

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0120	300.0	2203.9	10000	20.0	5.388	92.012	175.4	600.0	0.2923	8576	301.0720	0.02382	602.14	60214	3.411E-3	0.0	1.5
2.0120	300.0	2196.8	10000	20.0	5.380	93.012	174.8	600.0	0.2914	8563	549.7030	0.02379	1099.4	1.0994E5	3.411E-3	0.0	1.6
3.0040	300.0	2208.2	10000	20.0	5.383	94.004	175.7	600.0	0.2929	8567	928.3450	0.02380	1856.7	1.8567E5	3.411E-3	0.1	1.6
3.9960	300.0	2217.8	10000	20.0	5.375	94.996	176.5	600.0	0.2942	8555	1179.6700	0.02377	2359.3	2.3593E5	3.411E-3	0.1	1.6
5.0120	300.0	2213.2	10000	20.0	5.377	96.012	176.1	600.0	0.2935	8558	1445.2000	0.02377	2890.4	2.8904E5	3.411E-3	0.1	1.6
6.0000	300.0	2193.0	10000	20.0	5.408	97.000	174.5	600.0	0.2909	8608	1810.4301	0.02391	3620.9	3.6209E5	3.411E-3	0.1	1.6
7.0120	300.0	2225.2	10000	20.0	5.397	98.012	177.1	600.0	0.2951	8590	2057.7800	0.02386	4115.6	4.1156E5	3.411E-3	0.1	1.6
8.0040	300.0	2221.7	10000	20.0	5.393	99.004	176.8	600.0	0.2946	8583	2435.8000	0.02384	4871.6	4.8716E5	3.411E-3	0.1	1.7
9.0160	300.0	2208.7	10000	20.0	5.394	100.016	175.8	600.0	0.2930	8584	2686.1399	0.02385	5372.3	5.3723E5	3.411E-3	0.2	1.7
10.012	300.0	2203.0	10000	20.0	5.374	101.012	175.3	600.1	0.2921	8553	2937.4600	0.02375	5874.9	5.8749E5	3.411E-3	0.2	1.7
10.996	300.0	2212.7	10000	20.0	5.388	101.996	176.1	600.0	0.2935	8575	3317.1699	0.02382	6634.3	6.6343E5	3.411E-3	0.2	1.7
12.012	300.0	2218.6	10000	20.0	5.377	103.012	176.5	600.0	0.2943	8558	3565.8799	0.02377	7131.8	7.1318E5	3.411E-3	0.2	1.7
13.008	300.0	2208.9	10000	20.0	5.386	104.008	175.8	600.0	0.2930	8571	3819.2900	0.02381	7638.6	7.6386E5	3.411E-3	0.2	1.7
14.012	300.0	2200.3	10000	20.0	5.397	105.012	175.1	600.0	0.2918	8590	4194.3301	0.02386	8388.7	8.3887E5	3.411E-3	0.2	1.8
14.996	300.0	2216.2	10000	20.0	5.379	105.996	176.4	600.0	0.2939	8561	4445.4399	0.02378	8890.9	8.8909E5	3.411E-3	0.2	1.8
16.012	300.0	2208.1	10000	20.0	5.393	107.012	175.7	600.0	0.2929	8583	4822.5298	0.02384	9645.1	9.6451E5	3.411E-3	0.3	1.8
17.016	300.0	2208.7	10000	20.0	5.387	108.016	175.8	600.0	0.2929	8574	5074.0098	0.02382	10148	1.0148E6	3.411E-3	0.3	1.8
18.012	300.0	2205.2	10000	20.0	5.385	109.012	175.5	600.0	0.2925	8570	5324.9702	0.02381	10650	1.0650E6	3.411E-3	0.3	1.8
19.012	300.0	2198.9	10000	20.0	5.381	110.012	175.0	600.0	0.2916	8564	5703.9302	0.02379	11408	1.1408E6	3.411E-3	0.3	1.8
19.996	300.0	2202.3	10000	20.0	5.380	110.996	175.3	600.0	0.2921	8562	5953.2598	0.02378	11907	1.1907E6	3.411E-3	0.3	1.8
20.996	300.0	2224.8	10000	20.0	5.391	111.996	177.0	600.0	0.2951	8580	6333.7002	0.02383	12667	1.2667E6	3.411E-3	0.3	1.9
21.996	300.0	2205.0	10000	20.0	5.383	112.996	175.5	600.0	0.2924	8567	6581.6699	0.02380	13163	1.3163E6	3.411E-3	0.4	1.9
23.012	300.0	2205.0	10000	20.0	5.384	114.012	175.5	600.0	0.2924	8568	6833.1001	0.02380	13666	1.3666E6	3.411E-3	0.4	1.9
23.996	300.0	2221.0	10000	20.0	5.387	114.996	176.7	600.0	0.2946	8574	7212.1401	0.02382	14424	1.4424E6	3.411E-3	0.4	1.9
25.012	300.0	2220.5	10000	20.0	5.391	116.012	176.7	600.0	0.2945	8580	7461.2202	0.02383	14922	1.4922E6	3.411E-3	0.4	1.9
26.012	300.0	2202.0	10000	20.0	5.384	117.012	175.2	600.0	0.2920	8569	7713.8599	0.02380	15428	1.5428E6	3.411E-3	0.4	2.0
27.012	300.0	2224.0	10000	20.0	5.373	118.012	177.0	600.0	0.2950	8551	8093.9199	0.02375	16188	1.6188E6	3.411E-3	0.5	2.0
28.012	300.0	2204.5	10000	20.0	5.394	119.012	175.4	600.0	0.2924	8586	8342.4297	0.02385	16685	1.6685E6	3.411E-3	0.5	2.0
29.012	300.0	2205.3	10000	20.0	5.374	120.012	175.5	600.0	0.2925	8553	8721.5498	0.02376	17443	1.7443E6	3.411E-3	0.5	2.0
30.012	300.0	2189.8	10000	20.0	5.378	121.012	174.3	600.0	0.2904	8559	8969.6299	0.02377	17939	1.7939E6	3.411E-3	0.5	2.0
31.004	300.0	2203.0	10000	20.0	5.390	122.004	175.3	600.0	0.2922	8578	9220.7500	0.02383	18442	1.8442E6	3.411E-3	0.5	2.0
32.016	300.0	2224.0	10000	20.0	5.380	123.016	177.0	600.0	0.2950	8562	9598.8203	0.02378	19198	1.9198E6	3.411E-3	0.5	2.1
33.012	300.0	2221.7	10000	20.0	5.373	124.012	176.8	600.0	0.2947	8551	9851.4102	0.02375	19703	1.9703E6	3.411E-3	0.6	2.1
34.000	300.0	2216.8	10000	20.0	5.389	125.000	176.4	600.0	0.2940	8577	10227.900	0.02382	20456	2.0456E6	3.411E-3	0.6	2.1
34.996	300.0	2211.3	10000	20.0	5.381	125.996	176.0	599.9	0.2933	8564	10477.200	0.02379	20954	2.0954E6	3.411E-3	0.6	2.1
36.008	300.0	2201.3	10000	20.0	5.385	127.008	175.2	600.0	0.2920	8571	10729.700	0.02381	21459	2.1459E6	3.411E-3	0.6	2.1
37.012	300.0	2217.0	10000	20.0	5.390	128.012	176.4	600.0	0.2940	8578	11110.700	0.02383	22221	2.2221E6	3.411E-3	0.6	2.1
38.012	300.0	2210.1	10000	20.0	5.371	129.012	175.9	600.0	0.2931	8549	11359.300	0.02375	22719	2.2719E6	3.411E-3	0.6	2.2
38.996	300.0	2203.3	10000	20.0	5.369	129.996	175.3	600.0	0.2922	8546	11741.300	0.02374	23483	2.3483E6	3.411E-3	0.6	2.2
39.996	300.0	2196.0	10000	20.0	5.387	130.996	174.8	600.0	0.2912	8574	11985.200	0.02381	23970	2.3970E6	3.411E-3	0.7	2.2
40.996	300.0	2216.5	10000	20.0	5.384	131.996	176.4	600.0	0.2940	8569	12236.600	0.02380	24473	2.4473E6	3.411E-3	0.7	2.2
42.012	300.0	2205.3	10000	20.0	5.383	133.012	175.5	600.0	0.2925	8567	12615.700	0.02380	25231	2.5231E6	3.411E-3	0.7	2.2
43.012	300.0	2186.0	10000	20.0	5.391	134.012	174.0	600.0	0.2899	8579	12866.300	0.02383	25733	2.5733E6	3.411E-3	0.7	2.2
43.992	300.0	2209.5	10000	20.0	5.400	134.992	175.8	600.0	0.2931	8595	13117.900	0.02387	26236	2.6236E6	3.411E-3	0.7	2.2
45.012	300.0	2207.4	10000	20.0	5.409	136.012	175.7	600.0	0.2928	8608	13508.500	0.02391	27017	2.7017E6	3.411E-3	0.8	2.3
45.996	300.0	2196.9	10000	20.0	5.395	136.996	174.8	600.0	0.2914	8587	13744.400	0.02385	27489	2.7489E6	3.411E-3	0.8	2.3
46.996	300.0	2214.1	10000	20.0	5.379	137.996	176.2	600.0	0.2937	8561	14124.800	0.02378	28250	2.8250E6	3.411E-3	0.8	2.3
48.012	300.0	2205.0	10000	20.0	5.404	139.012	175.5	600.1	0.2924	8601	14372.900	0.02389	28746	2.8746E6	3.411E-3	0.8	2.3
48.996	300.0	2228.2	10000	20.0	5.386	139.996	177.3	599.9	0.2956	8572	14624.100	0.02382	29248	2.9248E6	3.411E-3	0.8	2.3
50.012	300.0	2217.0	10000	20.0	5.380	141.012	176.4	600.0	0.2940	8563	15003.800	0.02378	30008	3.0008E6	3.411E-3	0.8	2.4
50.996	300.0	2224.9	10000	20.0	5.386	141.996	177.1	599.9	0.2951	8572	15253.700	0.02382	30507	3.0507E6	3.411E-3	0.8	2.4
52.012	300.0	2202.1	10000	20.0	5.384	143.012	175.2	600.0	0.2921	8569	15629.300	0.02380	31259	3.1259E6	3.411E-3	0.9	2.4
53.012	300.0	2194.9	10000	20.0	5.383	144.012	174.7	600.0	0.2911	8567	15881.200	0.02380	31762	3.1762E6	3.411E-3	0.9	2.4
54.000	300.0	2216.5	10000	20.0	5.364	145.000	176.4	600.0	0.2940	8537	16132.200	0.02371	32264	3.2264E6	3.411E-3	0.9	2.4
54.996	300.0	2218.2	10000	20.0	5.379	145.996	176.5	600.0	0.2942	8561	16511.699	0.02378	33023	3.3023E6	3.411E-3	0.9	2.4
56.012	300.0	2202.0	10000	20.0	5.400	147.012	175.2	600.0	0.2920	8594	16760.500	0.02387	33521	3.3521E6	3.411E-3	0.9	2.5
56.996	300.0	2224.3	10000	20.0	5.408	147.996	177.0	600.0	0.2950	8607	17013.100	0.02391	34026	3.4026E6	3.411E-3	0.9	2.5
58.000	300.0	2209.8	10000	20.0	5.377	149.000	175.9	600.0	0.2931	8557	17388.801	0.02377	34778	3.4778E6	3.411E-3	1.0	2.5
58.996	300.0	2212.6	10000	20.0	5.384	149.996	176.1	600.0	0.2935	8568	17639.900	0.02380	35280	3.5280E6	3.411E-3	1.0	2.5
59.996	300.0	2211.1	10000	20.0	5.386	150.996	176.0	600.0	0.2932	8572	18017.100	0.02381	36034	3.6034E6	3.411E-3	1.0	2.5

Continuous ramp step 2

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0040	297.1	2184.3	10000	20.0	5.383	152.004	173.8	594.3	0.2925	8567	255.2720	0.02426	510.54	51054	3.411E-3	0.0	2.5
2.0200	291.1	2106.7	10000	20.0	5.403	153.020	167.6	582.3	0.2879	8598	613.1040	0.02536	1226.2	1.2262E5	3.411E-3	0.0	2.6
3.0200	287.1	2058.7	10000	20.0	5.406	154.020	163.8	574.2	0.2853	8604	859.7410	0.02610	1719.5	1.7195E5	3.411E-3	0.1	2.6
4.0200	282.9	2014.7	10000	20.0	5.427	155.020	160.3	565.9	0.2833	8637	1089.2100	0.02697	2178.4	2.1784E5	3.411E-3	0.1	2.6
5.0040	276.9	1942.1	10000	20.0	5.437	156.004	154.5	553.8	0.2791	8654	1426.2700	0.02822	2852.5	2.8525E5	3.411E-3	0.1	2.6
6.0280	272.9	1902.5	10000	20.0	5.439	157.028	151.4	545.7	0.2774	8656	1651.6600	0.02907	3303.3	3.3033E5	3.411E-3	0.1	2.6
7.0200	266.6	1832.7	10000	20.0	5.461	158.020	145.8	533.3	0.2735	8691	1989.7300	0.03056	3979.5	3.9795E5	3.411E-3	0.1	2.6
8.0200	262.6	1786.8	10000	20.0	5.481	159.020	142.2	525.2	0.2707	8723	2202.4600	0.03163	4404.9	4.4049E5	3.411E-3	0.1	2.7
9.0240	256.5	1734.5	10000	20.0	5.495	160.024	138.0	513.0	0.2691	8745	2521.7900	0.03323	5043.6	5.0436E5	3.411E-3	0.2	2.7
10.004	252.4	1676.9	10000	20.0	5.500	161.004	133.4	504.7	0.2644	8753	2734.5500	0.03436	5469.1	5.4691E5	3.411E-3	0.2	2.7
11.028	248.3	1651.1	10000	20.0	5.511	162.028	131.4	496.7	0.2645	8771	2934.8101	0.03555	5869.6	5.8696E5	3.411E-3	0.2	2.7
12.000	242.3	1596.6	10000	20.0	5.528	163.000	127.1	484.6	0.2622	8799	3235.2800	0.03747	6470.6	6.4706E5	3.411E-3	0.2	2.7
13.024	238.2	1532.4	10000	20.0	5.539	164.024	121.9	476.3	0.2560	8815	3435.5400	0.03885	6871.1	6.8711E5	3.411E-3	0.2	2.7
14.008	232.0	1473.7	10000	20.0	5.550	165.008	117.3	464.1	0.2527	8833	3723.3601	0.04101	7446.7	7.4467E5	3.411E-3	0.2	2.8
15.020	228.0	1440.1	10000	20.0	5.558	166.020	114.6	455.9	0.2514	8845	3911.2000	0.04255	7822.4	7.8224E5	3.411E-3	0.3	2.8
16.028	221.8	1382.8	10000	20.0	5.568	167.028	110.0	443.5	0.2481	8862	4192.5200	0.04505	8385.0	8.3850E5	3.411E-3	0.3	2.8
17.004	217.6	1342.3	10000	20.0	5.587	168.004	106.8	435.3	0.2454	8892	4373.9199	0.04694	8747.8	8.7478E5	3.411E-3	0.3	2.8
18.016	213.6	1302.0	10000	20.0	5.590	169.016	103.6	427.2	0.2425	8896	4549.0601	0.04874	9098.1	9.0981E5	3.411E-3	0.3	2.8
19.020	207.4	1236.7	10000	20.0	5.605	170.020	98.41	414.9	0.2372	8920	4811.7700	0.05183	9623.5	9.6235E5	3.411E-3	0.3	2.8
20.020	203.3	1205.1	10000	20.0	5.603	171.020	95.90	406.6	0.2359	8918	4980.6602	0.05395	9961.3	9.9613E5	3.411E-3	0.3	2.9
21.028	197.3	1146.4	10000	20.0	5.625	172.028	91.23	394.5	0.2312	8953	5224.4600	0.05752	10449	1.0449E6	3.411E-3	0.4	2.9
22.004	193.1	1113.7	10000	20.0	5.610	173.004	88.63	386.3	0.2295	8929	5386.9702	0.05985	10774	1.0774E6	3.411E-3	0.4	2.9
23.020	188.9	1069.3	10000	20.0	5.625	174.020	85.09	377.8	0.2252	8952	5550.3301	0.06271	11101	1.1101E6	3.411E-3	0.4	2.9
24.020	182.8	1015.4	10000	20.0	5.650	175.020	80.80	365.7	0.2210	8992	5774.6001	0.06724	11549	1.1549E6	3.411E-3	0.4	2.9
25.004	178.7	987.25	10000	20.0	5.656	176.004	78.56	357.5	0.2198	9001	5924.5801	0.07045	11849	1.1849E6	3.411E-3	0.4	2.9
26.028	172.4	926.95	10000	20.0	5.659	177.028	73.76	344.8	0.2139	9007	6149.8501	0.07577	12300	1.2300E6	3.411E-3	0.4	3.0
27.020	168.3	901.69	10000	20.0	5.667	178.020	71.75	336.6	0.2132	9020	6286.9600	0.07962	12574	1.2574E6	3.411E-3	0.5	3.0
28.020	164.2	861.75	10000	20.0	5.678	179.020	68.58	328.4	0.2088	9036	6427.5898	0.08378	12855	1.2855E6	3.411E-3	0.5	3.0
29.004	157.9	803.91	10000	20.0	5.685	180.004	63.97	315.7	0.2026	9048	6630.5098	0.09077	13261	1.3261E6	3.411E-3	0.5	3.0
30.020	153.8	780.95	10000	20.0	5.699	181.020	62.15	307.6	0.2020	9070	6756.1401	0.09586	13512	1.3512E6	3.411E-3	0.5	3.0
31.028	147.7	732.59	10000	20.0	5.705	182.028	58.30	295.3	0.1974	9080	6942.6699	0.1041	13885	1.3885E6	3.411E-3	0.5	3.0
32.020	143.4	689.56	10000	20.0	5.714	183.020	54.87	286.8	0.1913	9094	7068.1602	0.1106	14136	1.4136E6	3.411E-3	0.5	3.1
33.008	139.1	664.25	10000	20.0	5.716	184.008	52.86	278.3	0.1900	9097	7186.0298	0.1175	14372	1.4372E6	3.411E-3	0.6	3.1
34.016	133.0	617.23	10000	20.0	5.728	185.016	49.12	266.0	0.1846	9116	7355.5898	0.1288	14711	1.4711E6	3.411E-3	0.6	3.1
35.020	128.8	582.92	10000	20.0	5.732	186.020	46.39	257.5	0.1801	9123	7466.6899	0.1376	14933	1.4933E6	3.411E-3	0.6	3.1
36.004	124.5	560.31	10000	20.0	5.741	187.004	44.59	249.0	0.1791	9137	7573.4399	0.1474	15147	1.5147E6	3.411E-3	0.6	3.1
37.020	118.4	508.86	10000	20.0	5.754	188.020	40.49	236.8	0.1710	9158	7722.4702	0.1633	15445	1.5445E6	3.411E-3	0.6	3.1
38.020	114.2	481.01	10000	20.0	5.756	189.020	38.28	228.3	0.1677	9162	7822.0000	0.1758	15644	1.5644E6	3.411E-3	0.6	3.2
39.020	109.7	458.79	10000	20.0	5.766	190.020	36.51	219.5	0.1663	9177	7922.1499	0.1905	15844	1.5844E6	3.411E-3	0.7	3.2
40.020	103.5	413.07	10000	20.0	5.768	191.020	32.87	207.1	0.1588	9180	8053.2002	0.2141	16106	1.6106E6	3.411E-3	0.7	3.2
41.036	99.27	388.90	10000	20.0	5.780	192.036	30.95	198.5	0.1559	9199	8139.5098	0.2334	16279	1.6279E6	3.411E-3	0.7	3.2
42.020	94.83	358.90	10000	20.0	5.782	193.020	28.56	189.7	0.1506	9202	8226.5498	0.2558	16453	1.6453E6	3.411E-3	0.7	3.2
43.020	88.62	320.64	10000	20.0	5.789	194.020	25.52	177.2	0.1440	9214	8338.4502	0.2933	16677	1.6677E6	3.411E-3	0.7	3.2
44.020	84.35	297.65	10000	20.0	5.794	195.020	23.69	168.7	0.1404	9221	8412.9404	0.3240	16826	1.6826E6	3.411E-3	0.7	3.3
45.004	79.86	272.56	10000	20.0	5.800	196.004	21.69	159.7	0.1358	9232	8487.3203	0.3618	16975	1.6975E6	3.411E-3	0.8	3.3
46.024	75.32	251.84	10000	20.0	5.807	197.024	20.04	150.6	0.1330	9243	8589.4404	0.4073	17179	1.7179E6	3.411E-3	0.8	3.3
47.008	68.93	214.02	10000	20.0	5.814	198.008	17.03	137.9	0.1235	9253	8648.5098	0.4868	17297	1.7297E6	3.411E-3	0.8	3.3
48.016	64.33	195.41	10000	20.0	5.821	199.016	15.55	128.7	0.1209	9264	8710.2598	0.5596	17421	1.7421E6	3.411E-3	0.8	3.3
49.012	59.65	171.75	10000	20.0	5.821	200.012	13.67	119.3	0.1146	9264	8766.1699	0.6508	17532	1.7532E6	3.411E-3	0.8	3.3
50.020	55.40	153.98	10000	20.0	5.827	201.020	12.25	110.8	0.1106	9274	8815.1699	0.7554	17630	1.7630E6	3.411E-3	0.8	3.4
51.028	50.80	134.49	10000	20.0	5.829	202.028	10.70	101.6	0.1053	9277	8864.6104	0.8986	17729	1.7729E6	3.411E-3	0.9	3.4
52.020	44.07	106.75	10000	20.0	5.830	203.020	8.495	88.14	0.09638	9279	8925.8896	1.194	17852	1.7852E6	3.411E-3	0.9	3.4
53.020	39.72	91.307	10000	20.0	5.833	204.020	7.266	79.43	0.09148	9284	8962.6299	1.472	17925	1.7925E6	3.411E-3	0.9	3.4
54.024	34.85	72.823	10000	20.0	5.838	205.024	5.795	69.70	0.08314	9291	8999.0801	1.913	17998	1.7998E6	3.411E-3	0.9	3.4
55.004	29.75	56.471	10000	20.0	5.842	206.004	4.494	59.51	0.07552	9298	9029.3496	2.626	18059	1.8059E6	3.411E-3	0.9	3.4
56.028	25.40	44.464	10000	20.0	5.838	207.028	3.538	50.79	0.06966	9292	9053.4902	3.602	18107	1.8107E6	3.411E-3	0.9	3.5
57.004	20.20	31.084	10000	20.0	5.844	208.004	2.474	40.41	0.06121	9301	9077.1396	5.696	18154	1.8154E6	3.411E-3	1.0	3.5
58.004	14.42	18.062	10000	20.0	5.845	209.004	1.437	28.83	0.04985	9302	9094.5303	11.19	18189	1.8189E6	3.411E-3	1.0	3.5
59.020	9.647	8.9023	10000	20.0	5.849	210.020	0.7084	19.29	0.03672	9309	9105.8701	25.01	18212	1.8212E6	3.411E-3	1.0	3.5
60.020	6.315	3.9055	10000	20.0	5.847	211.020	0.3108	12.63	0.02461	9306	9110.6504	58.33	18221	1.8221E6	3.411E-3	1.0	3.5

